A review of redox analytical methods

A. D. Burnham; L. A. Miller; M. Roskosz

doi:10.1016/B978-0-323-99762-1.00117-0

A review of redox analytical methods

Research output: Chapter in Book/Report/Conference proceeding › Chapter › peer-review

Abstract

Measurements of the redox state of Earth and planetary materials require a very different set of techniques from those used to quantify elemental concentrations and isotopic ratios. Here, we review X-ray absorption near edge structure (XANES) and Mossbauer spectroscopies, from the fundamental theoretical principles underpinning the techniques to the practicalities of conduction an analysis and interpreting the data. In addition we discuss a handful of other relevant techniques.

Original language	English
Title of host publication	Treatise on Geochemistry, Third Edition, 8 Volume Set
Publisher	Elsevier
Pages	V8:255-V8:291
Volume	8
ISBN (Electronic)	9780323997638
ISBN (Print)	9780323997621
DOIs	https://doi.org/10.1016/B978-0-323-99762-1.00117-0
Publication status	Published - 1 Jan 2024

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abstract = "Measurements of the redox state of Earth and planetary materials require a very different set of techniques from those used to quantify elemental concentrations and isotopic ratios. Here, we review X-ray absorption near edge structure (XANES) and Mossbauer spectroscopies, from the fundamental theoretical principles underpinning the techniques to the practicalities of conduction an analysis and interpreting the data. In addition we discuss a handful of other relevant techniques.",

keywords = "EXAFS, M{\"o}ssbauer spectroscopy, Oxidation state, Oxygen fugacity, Redox state, Synchrotron, X-ray absorption spectroscopy, XANES, XAS",

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T1 - A review of redox analytical methods

AU - Burnham, A. D.

AU - Miller, L. A.

AU - Roskosz, M.

PY - 2024/1/1

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N2 - Measurements of the redox state of Earth and planetary materials require a very different set of techniques from those used to quantify elemental concentrations and isotopic ratios. Here, we review X-ray absorption near edge structure (XANES) and Mossbauer spectroscopies, from the fundamental theoretical principles underpinning the techniques to the practicalities of conduction an analysis and interpreting the data. In addition we discuss a handful of other relevant techniques.

AB - Measurements of the redox state of Earth and planetary materials require a very different set of techniques from those used to quantify elemental concentrations and isotopic ratios. Here, we review X-ray absorption near edge structure (XANES) and Mossbauer spectroscopies, from the fundamental theoretical principles underpinning the techniques to the practicalities of conduction an analysis and interpreting the data. In addition we discuss a handful of other relevant techniques.

KW - EXAFS

KW - Mössbauer spectroscopy

KW - Oxidation state

KW - Oxygen fugacity

KW - Redox state

KW - Synchrotron

KW - X-ray absorption spectroscopy

KW - XANES

KW - XAS

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U2 - 10.1016/B978-0-323-99762-1.00117-0

DO - 10.1016/B978-0-323-99762-1.00117-0

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AN - SCOPUS:85218397898

SN - 9780323997621

VL - 8

SP - V8:255-V8:291

BT - Treatise on Geochemistry, Third Edition, 8 Volume Set

PB - Elsevier

ER -

A review of redox analytical methods

Abstract

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