Full tip imaging in atom probe tomography

Sichao Du, Timothy Burgess, Shyeh Tjing Loi, Baptiste Gault, Qiang Gao, Peite Bao, Li Li, Xiangyuan Cui, Wai Kong Yeoh, Hark Hoe Tan, Chennupati Jagadish, Simon P. Ringer, Rongkun Zheng*

*Corresponding author for this work

    Research output: Contribution to journalArticlepeer-review

    24 Citations (Scopus)

    Abstract

    Atom probe tomography (APT) is capable of simultaneously revealing the chemical identities and three dimensional positions of individual atoms within a needle-shaped specimen, but suffers from a limited field-of-view (FOV), i.e., only the core of the specimen is effectively detected. Therefore, the capacity to analyze the full tip is crucial and much desired in cases that the shell of the specimen is also the region of interest. In this paper, we demonstrate that, in the analysis of III-V nanowires epitaxially grown from a substrate, the presence of the flat substrate positioned only micrometers away from the analyzed tip apex alters the field distribution and ion trajectories, which provides extra image compression that allows for the analysis of the entire specimen. An array of experimental results, including field desorption maps, elemental distributions, and crystallographic features clearly demonstrate the fact that the whole tip has been imaged, which is confirmed by electrostatic simulations.

    Original languageEnglish
    Pages (from-to)96-101
    Number of pages6
    JournalUltramicroscopy
    Volume124
    DOIs
    Publication statusPublished - Jan 2013

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