Abstract
Spark Plasma Sintering (SPS) method was practiced, in the current investigation, to obtain fully dense materials with an excellent dispersion of MWCNTs (Multi-walled Carbon Nanotubes) within the matrix. Scanning and transmission electron microscopy micrographs as well as Raman Spectroscopy revealed no conspicuous signs of damages on the nanotubes' structure, as a result of applying appropriate processing measures. Measurements of mechanical properties revealed the value of 15.2±0.4 MPa m1/2 for indentation fracture toughness, impling our success to align transformation toughening (while the zirconia has the grain size around 1 μm) with the effects of MWCNTs addition (5 wt%). High temperature mechanical properties of the composites have been investigated using Mechanical Spectroscopy (MS) up to 1600 K at frequency equal to 1 Hz. The MS results proved that CNTs could hinder grain-boundary sliding and subsequently lead to an enhanced creep resitance at high temperatures.
| Original language | English |
|---|---|
| Pages (from-to) | 3347-3352 |
| Number of pages | 6 |
| Journal | Ceramics International |
| Volume | 40 |
| Issue number | 2 |
| DOIs | |
| Publication status | Published - Mar 2014 |
| Externally published | Yes |
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