Studies in macrolide synthesis: Stereocontrolled synthesis of a C1-C13 segment of concanamycin A

Ian Paterson; Malcolm D. McLeod

doi:10.1016/S0040-4039(97)00816-2

Studies in macrolide synthesis: Stereocontrolled synthesis of a C₁-C₁₃ segment of concanamycin A

Ian Paterson^*, Malcolm D. McLeod

^*Corresponding author for this work

Research School of Chemistry

Research output: Contribution to journal › Article › peer-review

31 Citations (Scopus)

Abstract

The C₁-C₁₃ segment 6 of concanamycin A (1) was prepared by a highly stereocontrolled route (87% overall ds) in 16 steps from the ester 9. Key steps are the one-pot aldol/reduction, 8 → 12, and the HWE reaction, 18 + 19 → 6.

Original language	English
Pages (from-to)	4183-4186
Number of pages	4
Journal	Tetrahedron Letters
Volume	38
Issue number	23
DOIs	https://doi.org/10.1016/S0040-4039(97)00816-2
Publication status	Published - 9 Jun 1997

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title = "Studies in macrolide synthesis: Stereocontrolled synthesis of a C1-C13 segment of concanamycin A",

abstract = "The C1-C13 segment 6 of concanamycin A (1) was prepared by a highly stereocontrolled route (87\% overall ds) in 16 steps from the ester 9. Key steps are the one-pot aldol/reduction, 8 → 12, and the HWE reaction, 18 + 19 → 6.",

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AB - The C1-C13 segment 6 of concanamycin A (1) was prepared by a highly stereocontrolled route (87% overall ds) in 16 steps from the ester 9. Key steps are the one-pot aldol/reduction, 8 → 12, and the HWE reaction, 18 + 19 → 6.

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U2 - 10.1016/S0040-4039(97)00816-2

DO - 10.1016/S0040-4039(97)00816-2

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JO - Tetrahedron Letters

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IS - 23

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Studies in macrolide synthesis: Stereocontrolled synthesis of a C₁-C₁₃ segment of concanamycin A

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