Three- and five-quantum 17O MAS NMR of forsterite Mg2SiO4

Sharon E. Ashbrook; Andrew J. Berry; Stephen Wimperis

doi:10.2138/am-1999-7-824

Three- and five-quantum ¹⁷O MAS NMR of forsterite Mg₂SiO₄

Sharon E. Ashbrook
, Andrew J. Berry
, Stephen Wimperis^*

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

36 Citations (Scopus)

Abstract

Three- and five-quantum ¹⁷O MAS NMR experiments are used to resolve fully the three crystallographically distinct oxygen species in forsterite (Mg₂SiO₄). The chemical shift and quadrupolar parameters extracted from these spectra are compared with the literature values obtained using conventional ¹⁷O MAS and dynamic-angle-spinning (DAS) NMR.

Original language	English
Pages (from-to)	1191-1194
Number of pages	4
Journal	American Mineralogist
Volume	84
Issue number	7-8
DOIs	https://doi.org/10.2138/am-1999-7-824
Publication status	Published - 1999

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title = "Three- and five-quantum 17O MAS NMR of forsterite Mg2SiO4",

abstract = "Three- and five-quantum 17O MAS NMR experiments are used to resolve fully the three crystallographically distinct oxygen species in forsterite (Mg2SiO4). The chemical shift and quadrupolar parameters extracted from these spectra are compared with the literature values obtained using conventional 17O MAS and dynamic-angle-spinning (DAS) NMR.",

author = "Ashbrook, \{Sharon E.\} and Berry, \{Andrew J.\} and Stephen Wimperis",

year = "1999",

doi = "10.2138/am-1999-7-824",

language = "English",

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pages = "1191--1194",

journal = "American Mineralogist",

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TY - JOUR

T1 - Three- and five-quantum 17O MAS NMR of forsterite Mg2SiO4

AU - Ashbrook, Sharon E.

AU - Berry, Andrew J.

AU - Wimperis, Stephen

PY - 1999

Y1 - 1999

N2 - Three- and five-quantum 17O MAS NMR experiments are used to resolve fully the three crystallographically distinct oxygen species in forsterite (Mg2SiO4). The chemical shift and quadrupolar parameters extracted from these spectra are compared with the literature values obtained using conventional 17O MAS and dynamic-angle-spinning (DAS) NMR.

AB - Three- and five-quantum 17O MAS NMR experiments are used to resolve fully the three crystallographically distinct oxygen species in forsterite (Mg2SiO4). The chemical shift and quadrupolar parameters extracted from these spectra are compared with the literature values obtained using conventional 17O MAS and dynamic-angle-spinning (DAS) NMR.

UR - https://www.scopus.com/pages/publications/0033437204

U2 - 10.2138/am-1999-7-824

DO - 10.2138/am-1999-7-824

M3 - Article

SN - 0003-004X

VL - 84

SP - 1191

EP - 1194

JO - American Mineralogist

JF - American Mineralogist

IS - 7-8

ER -

Three- and five-quantum ¹⁷O MAS NMR of forsterite Mg₂SiO₄

Abstract

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