Vapour diffusion growth and characterisation of fully deuterated triglycine sulphate (ND 2CD 2COOD) 3D 2SO 4

J. M. Hudspeth; D. J. Goossens

doi:10.1016/j.jcrysgro.2011.11.002

Vapour diffusion growth and characterisation of fully deuterated triglycine sulphate (ND ₂CD ₂COOD) ₃D ₂SO ₄

J. M. Hudspeth^*, D. J. Goossens

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

6 Citations (Scopus)

Abstract

A new vial-in-vial vapour diffusion method for growing single crystals of fully deuterated triglycine sulphate (TGS) has been developed. Single crystals of hydrogenous TGS were also grown for comparison purposes. The crystals have been characterised using x-ray diffraction and differential scanning calorimetry. The phase transition temperature was 334.0±0.5 K for fully deuterated TGS compared to 322.3±0.3 K for hydrogenous TGS. These values compare well with the expected T _C.

Original language	English
Pages (from-to)	177-180
Number of pages	4
Journal	Journal of Crystal Growth
Volume	338
Issue number	1
DOIs	https://doi.org/10.1016/j.jcrysgro.2011.11.002
Publication status	Published - 1 Jan 2012

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10.1016/j.jcrysgro.2011.11.002

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title = "Vapour diffusion growth and characterisation of fully deuterated triglycine sulphate (ND 2CD 2COOD) 3D 2SO 4 ",

abstract = "A new vial-in-vial vapour diffusion method for growing single crystals of fully deuterated triglycine sulphate (TGS) has been developed. Single crystals of hydrogenous TGS were also grown for comparison purposes. The crystals have been characterised using x-ray diffraction and differential scanning calorimetry. The phase transition temperature was 334.0±0.5 K for fully deuterated TGS compared to 322.3±0.3 K for hydrogenous TGS. These values compare well with the expected T C.",

keywords = "A2. Single crystal growth, A2. Vapour diffusion-type crystallisation, B1. Fully deuterated triglycine sulphate, B3. Ferroelectric materials",

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AU - Hudspeth, J. M.

AU - Goossens, D. J.

PY - 2012/1/1

Y1 - 2012/1/1

N2 - A new vial-in-vial vapour diffusion method for growing single crystals of fully deuterated triglycine sulphate (TGS) has been developed. Single crystals of hydrogenous TGS were also grown for comparison purposes. The crystals have been characterised using x-ray diffraction and differential scanning calorimetry. The phase transition temperature was 334.0±0.5 K for fully deuterated TGS compared to 322.3±0.3 K for hydrogenous TGS. These values compare well with the expected T C.

AB - A new vial-in-vial vapour diffusion method for growing single crystals of fully deuterated triglycine sulphate (TGS) has been developed. Single crystals of hydrogenous TGS were also grown for comparison purposes. The crystals have been characterised using x-ray diffraction and differential scanning calorimetry. The phase transition temperature was 334.0±0.5 K for fully deuterated TGS compared to 322.3±0.3 K for hydrogenous TGS. These values compare well with the expected T C.

KW - A2. Single crystal growth

KW - A2. Vapour diffusion-type crystallisation

KW - B1. Fully deuterated triglycine sulphate

KW - B3. Ferroelectric materials

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DO - 10.1016/j.jcrysgro.2011.11.002

M3 - Article

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VL - 338

SP - 177

EP - 180

JO - Journal of Crystal Growth

JF - Journal of Crystal Growth

IS - 1

ER -

Vapour diffusion growth and characterisation of fully deuterated triglycine sulphate (ND ₂CD ₂COOD) ₃D ₂SO ₄

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